2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione

Base Information

• Chemical Name: 2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione
• CAS No.: 1446685-94-4
• Molecular Formula: C₃₆H₃₉N₃O₄
• Molecular Weight: 577.723
• Mol file: 1446685-94-4.mol

Synonyms:2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione

Chemical Property of 2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione

There total 1 articles about 2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-bromo-1,8-naphthalenedicarboxylic anhydride (81-86-7) + 2,6-diisopropylbenzenamine (24544-04-5) → 2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione (1446685-94-4)

Guidance literature:

4-bromo-1,8-naphthalenedicarboxylic anhydride; 2,6-diisopropylbenzenamine; for 24h; Heating;

With propionic acid; at 140 ℃; for 24h;

DOI:10.1016/j.jphotochem.2012.10.004

Reference yield: 54.0%

2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione (1446685-94-4) → 5-amino-2-[2,6-di(propan-2-yl)phenyl]-6-{[2,6-di(propan-2-yl)phenyl]amino}-1H-benzo[de]isoquinoline-1,3(2H)-dione

Guidance literature:

With sodium dithionite; In ethanol; water; for 3h; Reflux;

DOI:10.1016/j.molstruc.2016.07.018

Reference yield:

2-(2,6-diisopropylphenyl)-6-(2,6-diisopropylphenylamino)-5-nitro-1H-benzo[de]isoquinoline-1,3(2H)-dione (1446685-94-4) → 5,10-bis[2,6-di(propan-2-yl)phenyl]benzo[de]imidazo[4,5-g]isoquinoline-4,6(5H,10H)-dione

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dithionite / ethanol; water / 3 h / Reflux

2: methanesulfonic acid / 12 h

With sodium dithionite; methanesulfonic acid; In ethanol; water;

DOI:10.1016/j.molstruc.2016.07.018

upstream raw materials:

4-bromo-1,8-naphthalenedicarboxylic anhydride

2,6-diisopropylbenzenamine