Technology Process of C51H76O13
There total 3 articles about C51H76O13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; nickel(II) nitrate hexahydrate; oxygen; triethylamine; copper dichloride;
In
methanol;
at 60 ℃;
for 6h;
Microwave irradiation;
DOI:10.1002/chem.201203433
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: phosphorus tribromide / dichloromethane / 19 h / 0 - 20 °C
2.1: potassium carbonate; sodium iodide / dimethyl sulfoxide / 18 h / 50 °C
2.2: pH 2
3.1: nickel(II) nitrate hexahydrate; triethylamine; copper dichloride; pyridine; oxygen / methanol / 6 h / 60 °C / Microwave irradiation
With
pyridine; nickel(II) nitrate hexahydrate; oxygen; phosphorus tribromide; potassium carbonate; triethylamine; sodium iodide; copper dichloride;
In
methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/chem.201203433
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hydroxide / tetrahydrofuran; water / 18 h / 50 °C
2.1: potassium carbonate; sodium iodide / dimethyl sulfoxide / 18 h / 50 °C
2.2: pH 2
3.1: nickel(II) nitrate hexahydrate; triethylamine; copper dichloride; pyridine; oxygen / methanol / 6 h / 60 °C / Microwave irradiation
With
pyridine; nickel(II) nitrate hexahydrate; oxygen; potassium carbonate; triethylamine; sodium iodide; copper dichloride; lithium hydroxide;
In
tetrahydrofuran; methanol; water; dimethyl sulfoxide;
DOI:10.1002/chem.201203433
