Technology Process of C38H51NO6Si2
There total 5 articles about C38H51NO6Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 ℃;
for 0.333333h;
stereoselective reaction;
DOI:10.1002/anie.201008079
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ozone / dichloromethane / -78 °C
1.2: -78 - 20 °C
2.1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C
With
chloro-trimethyl-silane; titanium tetrachloride; ozone; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1002/anie.201008079
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 - 0 °C
2.1: ozone / dichloromethane / -78 °C
2.2: -78 - 20 °C
3.1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C
With
chloro-trimethyl-silane; oxalyl dichloride; titanium tetrachloride; ozone; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1002/anie.201008079