4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole

Base Information

Chemical Name:4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole
CAS No.:105471-07-6
Molecular Formula:C₂₀H₁₉N₅O₅
Molecular Weight:409.401
Hs Code.:

Synonyms:4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole

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Technology Process of 4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole

There total 4 articles about 4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 103022-65-7
4-cyano-5-p-cyanobenzoylamino-1-(5-O-p-cyanobenzoyl-2,3-O-isopropylidene-β-D-ribofuranosyl)imidazole

: 105471-07-6
4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole

Guidance literature:: With ammonium hydroxide; In ethanol; for 168h; Ambient temperature; 1M NaOH, MeOH, RT;

Reference yield:

: 362-75-4
2',3'-isopropylidene adenosine

: 105471-07-6
4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / Et₃N / CH₂Cl₂ / Ambient temperature

2: 93 percent / conc. NH₄OH / ethanol / 168 h / Ambient temperature; 1M NaOH, MeOH, RT

With ammonium hydroxide; triethylamine; In ethanol; dichloromethane;

Reference yield:

: 15888-38-7
5'-acetyl-2',3'-isopropylideneadenosine

: 105471-07-6
4-cyano-1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-5-(p-cyano-benzoylamino)imidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / pyridine

2: 8 percent / conc. NH₄OH / ethanol / 1.5 h / Ambient temperature

3: 53 percent / Et₃N / CH₂Cl₂ / Ambient temperature

4: 93 percent / conc. NH₄OH / ethanol / 168 h / Ambient temperature; 1M NaOH, MeOH, RT

With pyridine; ammonium hydroxide; triethylamine; In ethanol; dichloromethane;