methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate

Base Information

Chemical Name:methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate
CAS No.:1450736-52-3
Molecular Formula:C₂₈H₃₁ClO₂S
Molecular Weight:467.072
Hs Code.:

Synonyms:methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate

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Chemical Property of methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate

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Technology Process of methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate

There total 4 articles about methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1450736-51-2
methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)-6-hydroxyhexyl]thio}benzoate

: 1450736-52-3
methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 1450736-60-3
methyl 4-[(4-bromobutyl)thio]benzoate

: 1450736-52-3
methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium iodide / acetone / 6 h / 70 °C / Reflux

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

2.2: 90 °C

3.1: methanol; sodium tetrahydroborate / 2 h / 0 °C

4.1: triethylsilane; trifluoroacetic acid / dichloromethane / 20 °C

With methanol; triethylsilane; sodium tetrahydroborate; trifluoroacetic acid; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; acetone;

Reference yield:

: 1450736-50-1
methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)-6-oxohexyl]thio}benzoate

: 1450736-52-3
methyl 4-{[5-(3-chlorophenyl)-6-(3,4-dimethylphenyl)hexyl]thio}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium tetrahydroborate / 2 h / 0 °C

2: triethylsilane; trifluoroacetic acid / dichloromethane / 20 °C

With methanol; triethylsilane; sodium tetrahydroborate; trifluoroacetic acid; In dichloromethane;