-12-(phenylthio)-9-octadecenoic acid

Base Information

Chemical Name:-12-(phenylthio)-9-octadecenoic acid
CAS No.:123053-53-2
Molecular Formula:C₂₄H₃₈O₂S
Molecular Weight:390.631
Hs Code.:

<S-(E)>-12-(phenylthio)-9-octadecenoic acid

Synonyms:-12-(phenylthio)-9-octadecenoic acid

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Chemical Property of -12-(phenylthio)-9-octadecenoic acid

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Technology Process of -12-(phenylthio)-9-octadecenoic acid

There total 5 articles about -12-(phenylthio)-9-octadecenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 123053-52-1
methyl -12-(phenylthio)-9-octadecenoate

: 123053-53-2
-12-(phenylthio)-9-octadecenoic acid

Guidance literature:: With sodium hydroxide; In methanol; for 1.5h; Heating;
DOI:10.1021/jo00283a010

Reference yield:

: 141-22-0,27925-02-6,7431-95-0,84799-84-8
Ricinoleic acid

: 123053-53-2
-12-(phenylthio)-9-octadecenoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 34 percent / Ph₂S₂ / hexane / Irradiation

2: 95 percent / diethyl ether

3: 58 percent / pyridine / 40 h / Ambient temperature

4: 1.) sodium, methanol / 1.) RT, 30 min, 2.) MeOH, reflux, 3 h

5: 80 percent / 1 N aq. sodium hydroxide / methanol / 1.5 h / Heating

With pyridine; methanol; sodium hydroxide; sodium; diphenyldisulfane; In methanol; diethyl ether; hexane;
DOI:10.1021/jo00283a010

Reference yield:

: 540-12-5,27925-02-6,7431-95-0,84799-84-8
ricinelaidic acid

: 123053-53-2
-12-(phenylthio)-9-octadecenoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / diethyl ether

2: 58 percent / pyridine / 40 h / Ambient temperature

3: 1.) sodium, methanol / 1.) RT, 30 min, 2.) MeOH, reflux, 3 h

4: 80 percent / 1 N aq. sodium hydroxide / methanol / 1.5 h / Heating

With pyridine; methanol; sodium hydroxide; sodium; In methanol; diethyl ether;
DOI:10.1021/jo00283a010