(S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide

Base Information

Chemical Name:(S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide
CAS No.:578764-63-3
Molecular Formula:C₄₈H₄₀Br₂N₂O₆
Molecular Weight:900.663
Hs Code.:

Synonyms:(S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide

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Chemical Property of (S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide

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Technology Process of (S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide

There total 4 articles about (S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7533-40-6,14438-11-0
(S)-2-amino-4-methylpentan-1-ol

: 578764-63-3
(S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 5 h / 20 °C

2: 0.27 g / triphenylphosphine; diethyl azodicarboxylate / toluene / 22 h

3: TFA / CH₂Cl₂ / 4.5 h / 20 °C

4: 0.165 g / zinc acetate; imidazole / 2 h / 180 °C

With 1H-imidazole; zinc diacetate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; toluene; 2: Mitsunobu reaction;
DOI:10.1021/ja034926t

Reference yield:

: 82010-31-9
(S)-(1-hydroxymethyl-3-methylbutyl)carbamic acid tert-butyl ester

: 578764-63-3
(S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide

Guidance literature:: Multi-step reaction with 3 steps

1: 0.27 g / triphenylphosphine; diethyl azodicarboxylate / toluene / 22 h

2: TFA / CH₂Cl₂ / 4.5 h / 20 °C

3: 0.165 g / zinc acetate; imidazole / 2 h / 180 °C

With 1H-imidazole; zinc diacetate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In dichloromethane; toluene; 1: Mitsunobu reaction;
DOI:10.1021/ja034926t

Reference yield:

: 578764-69-9
(S)-[1-(4-bromophenoxymethyl)-3-methylbutyl]carbamic acid tert-butyl ester

: 578764-63-3
(S,S)-N,N'-bis[1-(4-bromophenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylicbisimide

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂ / 4.5 h / 20 °C

2: 0.165 g / zinc acetate; imidazole / 2 h / 180 °C

With 1H-imidazole; zinc diacetate; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ja034926t