6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

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Chemical Name:6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one
CAS No.:96555-40-7
Molecular Formula:C₃₁H₂₄BrN₅O₈
Molecular Weight:674.464
Hs Code.:

Synonyms:6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

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Chemical Property of 6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

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Technology Process of 6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

There total 3 articles about 6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 96575-35-8
6-amino-3-bromopyrazolo[3,4-d]pyrimidin-4(5H)-one

: 96555-41-8
C₃₁H₂₄BrN₅O₈

: 96555-40-7
6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

Guidance literature:: With boron trifluoride diethyl etherate; In nitromethane; for 1h; Heating;
DOI:10.1021/jm00146a007

Reference yield:

: 5334-26-9
6-(methylthio)pyrazolo<3,4-d>pyrimidin-4(5H)-one

: 96555-40-7
6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Br₂, CH₃COONa / H₂O / 0.5 h / 40 - 50 °C

2: 73 percent / aq. NH₄OH (conc.) / 16 h / 120 °C

3: 44 percent / BF₃*OEt₂ / nitromethane / 1 h / Heating

With ammonium hydroxide; boron trifluoride diethyl etherate; bromine; sodium acetate; In nitromethane; water;
DOI:10.1021/jm00146a007

Reference yield:

: 96555-39-4
3-bromo-4(5H)-oxopyrazolo[3,4-d]pyrimidin-6-yl methyl sulfoxide

: 96555-40-7
6-amino-3-bromo-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)pyrazolo<3,4-d>pyrimidin-4(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / aq. NH₄OH (conc.) / 16 h / 120 °C

2: 44 percent / BF₃*OEt₂ / nitromethane / 1 h / Heating

With ammonium hydroxide; boron trifluoride diethyl etherate; In nitromethane;
DOI:10.1021/jm00146a007