(E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:(E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide
CAS No.:1338091-91-0
Molecular Formula:C₁₉H₂₂N₂O₄S
Molecular Weight:374.461
Hs Code.:

Synonyms:(E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Suppliers and Price of (E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Chemical Property:

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Technology Process of (E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

There total 2 articles about (E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1338091-83-0
(E)-N′-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

: 106-95-6
allyl bromide

: 1338091-91-0
(E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: With caesium carbonate; at 20 ℃; for 1h; Neat (no solvent); Ball-milling;
DOI:10.1016/j.tet.2011.07.056

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1338091-91-0
(E)-N-allyl-N'-(3,5-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / 20 °C / Neat (no solvent); Ball-milling

2: caesium carbonate / 1 h / 20 °C / Neat (no solvent); Ball-milling

With caesium carbonate;
DOI:10.1016/j.tet.2011.07.056