C₆₃H₆₁BF₂N₄O

Base Information

• Chemical Name: C₆₃H₆₁BF₂N₄O
• CAS No.: 1470004-02-4
• Molecular Formula: C₆₃H₆₁BF₂N₄O
• Molecular Weight: 939.011
• Mol file: 1470004-02-4.mol

Synonyms:C₆₃H₆₁BF₂N₄O

Chemical Property of C₆₃H₆₁BF₂N₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₃H₆₁BF₂N₄O

There total 4 articles about C₆₃H₆₁BF₂N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

[4-[bis(4-methylphenyl)amino]phenyl]boronic acid (654067-65-9) + C23H25BBr2F2N2O → C63H61BF2N4O (1470004-02-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In water; toluene; at 90 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.08.088

Reference yield:

4-[(2-ethylhexyl)oxy]benzaldehyde (119630-71-6) → C63H61BF2N4O (1470004-02-4)

Guidance literature:

Multi-step reaction with 4 steps

1.1: indium(III) chloride / 4 h / 20 °C / Inert atmosphere

2.1: chloranil / dichloromethane / 8 h / 20 °C

2.2: 3 h / 20 °C / Inert atmosphere

3.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 6 h / Inert atmosphere; Reflux

4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 24 h / 90 °C / Inert atmosphere

With indium(III) chloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; chloranil; sodium carbonate; dibenzoyl peroxide; In tetrachloromethane; dichloromethane; water; toluene; 4.1: |Suzuki Coupling;

DOI:10.1016/j.tetlet.2013.08.088

Reference yield:

C23H27BF2N2O → C63H61BF2N4O (1470004-02-4)

Guidance literature:

Multi-step reaction with 2 steps

1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 6 h / Inert atmosphere; Reflux

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 24 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; dibenzoyl peroxide; In tetrachloromethane; water; toluene; 2: |Suzuki Coupling;

DOI:10.1016/j.tetlet.2013.08.088

upstream raw materials:

[4-[bis(4-methylphenyl)amino]phenyl]boronic acid

4-[(2-ethylhexyl)oxy]benzaldehyde