2,4,6-Trichlorobenzylidene dichloride

Base Information

• Chemical Name: 2,4,6-Trichlorobenzylidene dichloride
• CAS No.: 28744-45-8
• Molecular Formula: C₇H₃Cl₅
• Molecular Weight: 264.366
• Mol file: 28744-45-8.mol

Synonyms:2,4,6-Trichlorobenzylidene dichloride

Chemical Property of 2,4,6-Trichlorobenzylidene dichloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,6-Trichlorobenzylidene dichloride

There total 2 articles about 2,4,6-Trichlorobenzylidene dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,4,6-tribromotoluene (6320-40-7) → 2,4,6-Trichlorobenzylidene dichloride (28744-45-8)

Guidance literature:

With phosphorus trichloride; at 180 - 220 ℃; for 10h; Irradiation;

DOI:10.1007/BF00762032

Reference yield:

2,4,6-trichlorotoluene (23749-65-7) → 2,4,6-Trichlorobenzylidene dichloride (28744-45-8)

Guidance literature:

at 200 ℃; Einleiten von Chlor;

Reference yield:

2,4,6-Trichlorobenzylidene dichloride (28744-45-8) → 2,4,6-trichlorobenzaldehyde (24473-00-5)

Guidance literature:

With sulfuric acid;

upstream raw materials:

2,4,6-trichlorotoluene

2,4,6-tribromotoluene

Downstream raw materials:

2,4,6-trichlorobenzaldehyde

Refernces