Technology Process of C13H12FN5OS
There total 6 articles about C13H12FN5OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C6H7N5OS; 4-Fluorobenzyl bromide;
With
sodium hydroxide;
In
water;
at 0 - 26 ℃;
With
acetic acid;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: ISOPROPYLAMIDE / 6 h / 20 °C
1.2: 1 h / 100 °C
1.3: 0 °C / pH 8
2.1: pyridine / 3 h / 80 °C
3.1: N-chloro-succinimide; acetic acid / 6 h / 80 °C
4.1: thiourea / ethanol / 4 h / 80 °C
5.1: hydrogenchloride / water / 1 h / 60 °C
5.2: 0 °C / pH 8
6.1: sodium hydroxide / water / 0 - 26 °C
With
pyridine; hydrogenchloride; N-chloro-succinimide; acetic acid; thiourea; sodium hydroxide;
In
ethanol; ISOPROPYLAMIDE; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-chloro-succinimide; acetic acid / 6 h / 80 °C
2.1: thiourea / ethanol / 4 h / 80 °C
3.1: hydrogenchloride / water / 1 h / 60 °C
3.2: 0 °C / pH 8
4.1: sodium hydroxide / water / 0 - 26 °C
With
hydrogenchloride; N-chloro-succinimide; acetic acid; thiourea; sodium hydroxide;
In
ethanol; water;