3-(methylamino)-4-aminoacetophenone

Base Information

Chemical Name:3-(methylamino)-4-aminoacetophenone
CAS No.:92642-29-0
Molecular Formula:C₉H₁₂N₂O
Molecular Weight:164.207
Hs Code.:

Synonyms:3-(methylamino)-4-aminoacetophenone

Suppliers and Price of 3-(methylamino)-4-aminoacetophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(methylamino)-4-aminoacetophenone

Chemical Property:

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Technology Process of 3-(methylamino)-4-aminoacetophenone

There total 6 articles about 3-(methylamino)-4-aminoacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7463-31-2
3-Acetamidoacetophenone

: 92642-29-0
3-(methylamino)-4-aminoacetophenone

Guidance literature:: Multi-step reaction with 5 steps

1: nitric acid, acetic anhydride

2: KOH / ethanol; H₂O

3: 98 percent / trifluoroacetic anhydride / 0.42 h

4: 1.) K₂CO₃ / 1.) dimethoxyethane; 2.) r.t., overnight

5: hydrogen / 10percent palladium on charcoal / ethanol / 1 h

With potassium hydroxide; hydrogen; nitric acid; acetic anhydride; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In ethanol; water;
DOI:10.1021/ja00334a053

Reference yield:

: 79127-39-2
3-(methylamino)-4-nitroacetophenone

: 92642-29-0
3-(methylamino)-4-aminoacetophenone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 4h; Ambient temperature;
DOI:10.1021/ja00410a040

Reference yield:

: 79127-41-6
1-(3-amino-4-nitrophenyl)ethan-1-one

: 92642-29-0
3-(methylamino)-4-aminoacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / trifluoroacetic anhydride / 0.42 h

2: 1.) K₂CO₃ / 1.) dimethoxyethane; 2.) r.t., overnight

3: hydrogen / 10percent palladium on charcoal / ethanol / 1 h

With hydrogen; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In ethanol;
DOI:10.1021/ja00334a053