HEPTYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: HEPTYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE
• CAS No.: 115414-48-7
• Molecular Formula: C₁₅H₂₉NO₆
• Molecular Weight: 319.398
• Mol file: 115414-48-7.mol

Synonyms:HEPTYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE;HEPTYL 2-ACETAMIDO-2-DEOXY-SS-D-GLUCOPYRANOSIDE

Chemical Property of HEPTYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

Chemical Property:

• Boiling Point: 551.1±50.0 °C(Predicted)
• PKA: 13.00±0.70(Predicted)
• PSA: 108.25000
• Density: 1.18±0.1 g/cm3(Predicted)
• LogP: 0.30800

Purity/Quality:

98%min ^*data from raw suppliers

HEPTYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of HEPTYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

There total 3 articles about HEPTYL 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

heptyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside (115431-24-8) → heptyl 2-acetamido-2-deoxy-β-D-glucopyranoside (115414-48-7)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1007/BF00598682

Reference yield:

n-heptan1ol (111-70-6) → heptyl 2-acetamido-2-deoxy-β-D-glucopyranoside (115414-48-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / Heating

2: 84 percent / sodium methanolate / methanol

With sodium methylate; toluene-4-sulfonic acid; In methanol; 1,2-dichloro-ethane;

DOI:10.1007/BF00598682

Reference yield:

2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline (10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1) → heptyl 2-acetamido-2-deoxy-β-D-glucopyranoside (115414-48-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / Heating

2: 84 percent / sodium methanolate / methanol

With sodium methylate; toluene-4-sulfonic acid; In methanol; 1,2-dichloro-ethane;

DOI:10.1007/BF00598682

upstream raw materials:

heptyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

n-heptan1ol

2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

Downstream raw materials:

O-(heptyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosid-3-yl)-D-lactoyl-L-alanyl-D-isoglutamine γ-benzyl ester

O-(heptyl 2-acetamido-2-deoxy-β-D-glucopyranosid-3-yl)-D-lactoyl-L-alanyl-D-isoglutamine γ-benzyl ester

heptyl 2-acetamido-4,6-O-benzylidene-3-O-(D-1-carboxyethyl)-2-deoxy-β-D-glucopyranoside

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