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Technology Process of (aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2

(aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2

Base Information
  • Chemical Name:(aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2
  • CAS No.:609344-52-7
  • Molecular Formula:C60H74Al2I2
  • Molecular Weight:1103.02
  • Hs Code.:
(aluminum)2I<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>-2,6-(C<sub>6</sub>H<sub>3</sub>-2,6-iPr<sub>2</sub>)2)2

Synonyms:(aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2

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Chemical Property of (aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2
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Technology Process of (aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2

There total 2 articles about (aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(aluminum)I<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>-2,6-(C<sub>6</sub>H<sub>3</sub>-2,6-iPr<sub>2</sub>)2)

(aluminum)I2(C6H3-2,6-(C6H3-2,6-iPr2)2)

Bis(trimethylsilyl)ethyne
14630-40-1

Bis(trimethylsilyl)ethyne

(Al(CSi(CH<sub>3</sub>)3)(2,6-(2,6-(isopropyl)2C<sub>6</sub>H<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>))2
889470-28-4

(Al(CSi(CH3)3)(2,6-(2,6-(isopropyl)2C6H3)2C6H3))2

(aluminum)2I<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>-2,6-(C<sub>6</sub>H<sub>3</sub>-2,6-iPr<sub>2</sub>)2)2
609344-52-7

(aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2

Guidance literature:
With KC8; In toluene; a soln. of Al compd. and acetylene deriv. added to a suspn. of KC8 (2 equiv.), stirred at room temp. for 50 h, filtered, the filtrate concd., kept at 5°C overnight; filtered, the filtrate concd., stored at -30°C overnight; elem. anal.;
DOI:10.1002/anie.200504329

Reference yield: 40.0%

(aluminum)I<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>-2,6-(C<sub>6</sub>H<sub>3</sub>-2,6-iPr<sub>2</sub>)2)

(aluminum)I2(C6H3-2,6-(C6H3-2,6-iPr2)2)

(aluminum)2I<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>-2,6-(C<sub>6</sub>H<sub>3</sub>-2,6-iPr<sub>2</sub>)2)2
609344-52-7

(aluminum)2I2(C6H3-2,6-(C6H3-2,6-iPr2)2)2

Guidance literature:
With KC8; In diethyl ether; byproducts: KI; a soln. of complex in diethyl ether was added dropwise over 30 min to KC8 at ca. -78°C and stirred for 12 h; decanted from the graphite, ether was removed under reduced pressure, the residue was washed with hexane; elem. anal.;
DOI:10.1021/ja034478p
upstream raw materials:

Bis(trimethylsilyl)ethyne

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