5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Base Information

Chemical Name:5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone
CAS No.:172843-15-1
Molecular Formula:C₃₆H₅₄O₅Si
Molecular Weight:594.907
Hs Code.:

Synonyms:5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

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Technology Process of 5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

There total 6 articles about 5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: BH₃ *SMe₂

: 172843-13-9
2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

: 172843-15-1
5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Guidance literature:: With pyridinium chlorochromate; In tetrahydrofuran; hexane;

Reference yield:

: Tetradecanoic acid 2-(tert-butyl-diphenyl-silanyloxymethyl)-2,5-dihydroxy-pentyl ester

: 172843-15-1
5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 72h; Yield given; Ambient temperature;
DOI:10.1021/jm950276v

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 172843-15-1
5-<<(tert-butyldiphenylsilyl)oxy>methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / (dimethylamino)pyridine / pyridine / 16 h / Ambient temperature

2: 77 percent / DMAP, pyridine / CH₂Cl₂ / 24 h

3: 77 percent / TiCl₄ / CH₂Cl₂ / 0.67 h / Ambient temperature

4: BH₃*SMe₂ / tetrahydrofuran / 12 h / Ambient temperature

5: pyridinium chlorochromate / CH₂Cl₂ / 72 h / Ambient temperature

With pyridine; dmap; dimethylsulfide borane complex; titanium tetrachloride; pyridinium chlorochromate; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/jm950276v