12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester

Base Information

Chemical Name:12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester
CAS No.:343861-73-4
Molecular Formula:C₃₄H₆₀N₂O₆
Molecular Weight:592.86
Hs Code.:

Synonyms:12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester

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Chemical Property of 12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester

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Technology Process of 12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester

There total 9 articles about 12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77798-73-3
2,5-Bis<11-(methoxycarbonyl)undecyl>-3,6-dinitrohydrochinon-dimethylether

: 343861-73-4
12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester

Guidance literature:: With hydrogen; nickel; In benzene; at 80 ℃; for 5h; under 73550.8 Torr;

Reference yield:

: 1108-58-3
<10-(Methoxycarbonyl)decyl>triphenylphosphoniumiodid

: 343861-73-4
12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: NaOMe / dimethylformamide / 1) 0 deg C, 10 min, 2) r.t., 1.5 h

2: 70 percent / dimethylformamide / 3 h / Ambient temperature

3: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

4: 48percent HBr / acetic acid / 14 h / 110 °C

5: pyridine / 14 h / Ambient temperature

6: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

7: 8.2 g / H₂SO₃, SO₂ / acetic acid / 5 h / 80 °C

8: 58 percent / K₂CO₃ / acetone / 4 h / Heating

9: H₂ / Raney-Ni / benzene / 5 h / 80 °C / 73550.8 Torr

With sulfur dioxide; hydrogen bromide; hydrogen; nitric acid; sodium methylate; sulphurous acid; potassium carbonate; nickel; In pyridine; methanol; acetic acid; propionic acid; N,N-dimethyl-formamide; acetone; benzene;

Reference yield:

: 343859-17-6
12-[4-(11-Carboxy-undecyl)-2,5-dihydroxy-phenyl]-dodecanoic acid

: 343861-73-4
12-[2,5-Diamino-3,6-dimethoxy-4-(11-methoxycarbonyl-undecyl)-phenyl]-dodecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 14 h / Ambient temperature

2: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

3: 8.2 g / H₂SO₃, SO₂ / acetic acid / 5 h / 80 °C

4: 58 percent / K₂CO₃ / acetone / 4 h / Heating

5: H₂ / Raney-Ni / benzene / 5 h / 80 °C / 73550.8 Torr

With sulfur dioxide; hydrogen; nitric acid; sulphurous acid; potassium carbonate; nickel; In pyridine; acetic acid; propionic acid; acetone; benzene;