1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid benzhydryl ester

Base Information

• Chemical Name: 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid benzhydryl ester
• CAS No.: 101833-98-1
• Molecular Formula: C₂₉H₂₈N₂O₅S
• Molecular Weight: 516.618

Synonyms:1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid benzhydryl ester

Chemical Property of 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid benzhydryl ester

Chemical Property:

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Technology Process of 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid benzhydryl ester

There total 9 articles about 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

benzophenone hydrazone (5350-57-2) + 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ4-penicillanic acid (4052-54-4,34104-15-9,41399-39-7,52248-38-1,54773-98-7,72402-09-6) → 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ4-penicillanic acid benzhydryl ester (101833-98-1)

Guidance literature:

With aluminum oxide; Oxone; iodine; In dichloromethane; at 0 ℃; for 4.5h;

DOI:10.1016/S0040-4039(97)00046-4

Reference yield: 94.0%

(S)-3,3-Dimethyl-7-oxo-6-phenylacetylamino-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester (66363-41-5,67565-52-0) → (S)-3,3-Dimethyl-4,7-dioxo-6-phenylacetylamino-4λ4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester (37591-56-3,51446-87-8,68000-33-9,69780-17-2,73036-93-8,101833-98-1)

Guidance literature:

With formic acid; dihydrogen peroxide; In dichloromethane; at 0 - 5 ℃; for 4h;

DOI:10.1055/s-1989-27194

Reference yield: 63.0%

(2S,4R,5R,6R)-6-(Bis-phenylacetyl-amino)-3,3-dimethyl-4,7-dioxo-4λ4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester (101760-76-3) → benzyl 6β-(phenylacetamido)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo<3.2.0>heptane-2α-carboxylate 1α-S-oxide (37591-56-3,51446-87-8,68000-33-9,69780-17-2,73036-93-8,101833-98-1)

Guidance literature:

With ammonium acetate; zinc; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/jo00360a030

upstream raw materials:

benzophenone hydrazone

1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid

(S)-3,3-Dimethyl-7-oxo-6-phenylacetylamino-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

(2S,4R,5R,6R)-6-(Bis-phenylacetyl-amino)-3,3-dimethyl-4,7-dioxo-4λ⁴-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

Downstream raw materials:

(R)-2-((1S,5R)-3-Benzyl-7-oxo-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-methyl-but-3-enoic acid benzhydryl ester

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