5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine

Base Information

• Chemical Name: 5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine
• CAS No.: 113544-68-6
• Molecular Formula: C₃₇H₃₅N₃O₁₇S
• Molecular Weight: 825.761

Synonyms:5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine

Chemical Property of 5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine

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Technology Process of 5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine

There total 3 articles about 5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>-2',3'-O-isopropylideneuridine (113544-62-0,113567-40-1) → 5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine (113544-68-6)

Guidance literature:

With water; trifluoroacetic acid; for 0.5h; Ambient temperature;

DOI:10.1016/0223-5234(87)90174-7

Reference yield:

3,4,6-tri-O-benzoyl-2-deoxy-α,β-D-glucopyranose (101857-04-9,101857-07-2) → 5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine (113544-68-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) pyridine / 1.) methylene chloride, -20 to -15 deg C, 2.) methylene chloride, R_.T_., 20 h

2: 88 percent / trifluoroacetic acid, water / 0.5 h / Ambient temperature

With pyridine; water; trifluoroacetic acid;

DOI:10.1016/0223-5234(87)90174-7

Reference yield:

2',3'-O-isopropylideneuridine (362-43-6) → 5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>uridine (113544-68-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) pyridine / 1.) methylene chloride, -20 to -15 deg C, 2.) methylene chloride, R_.T_., 20 h

2: 88 percent / trifluoroacetic acid, water / 0.5 h / Ambient temperature

With pyridine; water; trifluoroacetic acid;

DOI:10.1016/0223-5234(87)90174-7

upstream raw materials:

5'-O-<<<<(3'',4'',6''-tri-O-benzoyl-2''-deoxy-α-D-glucopyranosyl)oxy>carbonyl>amino>sulfonyl>-2',3'-O-isopropylideneuridine

3,4,6-tri-O-benzoyl-2-deoxy-α,β-D-glucopyranose

2',3'-O-isopropylideneuridine

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