N,3-diphenylisoxazol-5-amine

Base Information

Chemical Name:N,3-diphenylisoxazol-5-amine
CAS No.:15055-49-9
Molecular Formula:C₁₅H₁₂N₂O
Molecular Weight:236.273
Hs Code.:

Synonyms:N,3-diphenylisoxazol-5-amine

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Chemical Property of N,3-diphenylisoxazol-5-amine

Chemical Property:

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Technology Process of N,3-diphenylisoxazol-5-amine

There total 5 articles about N,3-diphenylisoxazol-5-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: C₁₉H₂₀N₂

: 15055-49-9
N,3-diphenylisoxazol-5-amine

Guidance literature:: With hydroxylamine hydrochloride; In ethanol; at 100 ℃; for 0.5h;
DOI:10.1021/acs.orglett.9b03201

Reference yield:

: 62-53-3
aniline

: 15055-49-9
N,3-diphenylisoxazol-5-amine

Guidance literature:: Multi-step reaction with 4 steps

1: palladium dichloride; silver trifluoroacetate; potassium carbonate / acetonitrile / 4 h / 100 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C

3: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 24 h / 20 °C / Inert atmosphere

4: hydroxylamine hydrochloride / ethanol / 0.5 h / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; silver trifluoroacetate; potassium carbonate; triethylamine; palladium dichloride; In tetrahydrofuran; ethanol; acetonitrile; 3: |Sonogashira Cross-Coupling;
DOI:10.1021/acs.orglett.9b03201

Reference yield:

: (E)-N-(tert-butyl)-N'-phenyl-3-(triisopropylsilyl)propiolimidamide

: 15055-49-9
N,3-diphenylisoxazol-5-amine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 24 h / 20 °C / Inert atmosphere

3: hydroxylamine hydrochloride / ethanol / 0.5 h / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; ethanol; 2: |Sonogashira Cross-Coupling;
DOI:10.1021/acs.orglett.9b03201