(Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate

Base Information

Chemical Name:(Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate
CAS No.:1429782-56-8
Molecular Formula:C₁₇H₁₃NO₂S₂
Molecular Weight:327.428
Hs Code.:

Synonyms:(Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate

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Technology Process of (Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate

There total 2 articles about (Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 75-15-0,12122-00-8
carbon disulfide

: 159970-12-4
4-(2-aminophenylethynyl)benzoic acid methyl ester

: 1429782-56-8
(Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate

Guidance literature:: With sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 25 ℃; for 24h; Sealed tube; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.02.074

Reference yield:

: 615-43-0
2-iodophenylamine

: 3034-86-4
4-ethynylbenzoic acid methyl ester

: 1429782-56-8
(Z)-methyl 4-((2-mercapto-4H-benzo[d][1,3]thiazin-4-ylidene)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium-copper catalyst / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; sulfuric acid / acetonitrile / 24 h / 25 °C / Sealed tube; Inert atmosphere

With sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1016/j.tetlet.2013.02.074