C₂₅H₃₈O₇Si

Base Information

Chemical Name:C₂₅H₃₈O₇Si
CAS No.:1415904-96-9
Molecular Formula:C₂₅H₃₈O₇Si
Molecular Weight:478.658
Hs Code.:

C<sub>25</sub>H<sub>38</sub>O<sub>7</sub>Si

Synonyms:C₂₅H₃₈O₇Si

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Chemical Property of C₂₅H₃₈O₇Si

Chemical Property:

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Technology Process of C₂₅H₃₈O₇Si

There total 5 articles about C₂₅H₃₈O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415904-89-0
5-(((3aR,4R,6R,6aR)-6-((tert-butyldimethylsilyloxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylsulfonyl)-1-phenyl-1H-tetrazole

: 80241-82-3
methyl 2-formyl-6-methoxybenzoate

: 1415904-93-6
C₂₅H₃₈O₇Si

: 1415904-96-9
C₂₅H₃₈O₇Si

Guidance literature:: With lithium hexamethyldisilazane; In 1,2-dimethoxyethane; at -78 - 20 ℃; for 13.25h; Overall yield = 76 %; Overall yield = 1.02 g; stereoselective reaction;
DOI:10.1016/j.tetasy.2012.10.010

Reference yield:

: 73274-87-0,73713-38-9
3-hydroxy-7-methoxy-3H-isobenzofuran-1-one

: 1415904-93-6
C₂₅H₃₈O₇Si

: 1415904-96-9
C₂₅H₃₈O₇Si

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / 1.33 h / 0 °C

2: lithium hexamethyldisilazane / 1,2-dimethoxyethane / 13.25 h / -78 - 20 °C

With lithium hexamethyldisilazane; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; 2: |Julia-Kocienski Olefination;
DOI:10.1016/j.tetasy.2012.10.010

Reference yield:

: 188127-20-0
((3aS,4S,6R,6aR)-6-(((tert-butyldimethylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol

: 1415904-93-6
C₂₅H₃₈O₇Si

: 1415904-96-9
C₂₅H₃₈O₇Si

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2.5 h / 0 - 20 °C

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 12.17 h / 0 - 20 °C

3: lithium hexamethyldisilazane / 1,2-dimethoxyethane / 13.25 h / -78 - 20 °C

With hexaammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; 3: |Julia-Kocienski Olefination;
DOI:10.1016/j.tetasy.2012.10.010