4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate

Base Information

Chemical Name:4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate
CAS No.:1299470-40-8
Molecular Formula:C₂₄H₂₇FN₂O₄*H₃O₄P
Molecular Weight:524.483
Hs Code.:

Synonyms:4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate

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Chemical Property of 4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate

Chemical Property:

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Technology Process of 4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate

There total 5 articles about 4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133454-47-4
iloperidone

: 1299470-40-8
4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate

Guidance literature:: With phosphoric acid; In isopropyl alcohol; Reflux;

Reference yield:

: 58113-30-7
4-(3-chloropropoxy)-3-methoxyacetophenone

: 1299470-40-8
4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 60 - 85 °C

1.2: 0 - 30 °C

2.1: triethylamine / methanol

3.1: phosphoric acid / isopropyl alcohol / Reflux

With phosphoric acid; potassium carbonate; triethylamine; In methanol; isopropyl alcohol; acetonitrile;

Reference yield:

: 498-02-2
1-(3-methoxy-4-hydroxyphenyl)ethanone

: 1299470-40-8
4'-[3-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]propoxy]-3'-methoxyacetophenone phosphate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2.1: potassium carbonate / acetonitrile / 60 - 85 °C

2.2: 0 - 30 °C

3.1: triethylamine / methanol

4.1: phosphoric acid / isopropyl alcohol / Reflux

With phosphoric acid; potassium carbonate; triethylamine; In methanol; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;