Technology Process of C20H20FNO3
There total 5 articles about C20H20FNO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
C30H40Br2ClFeN2O2; silver perchlorate; N-fluorobis(benzenesulfon)imide;
In
diethyl ether;
at 0 ℃;
for 8h;
enantioselective reaction;
Inert atmosphere;
Molecular sieve;
DOI:10.1039/c4cc01631a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / -40 - 20 °C / Inert atmosphere
2: dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere
3: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C / Inert atmosphere
4: N-fluorobis(benzenesulfon)imide; silver perchlorate; C30H40Br2ClFeN2O2 / diethyl ether / 8 h / 0 °C / Inert atmosphere; Molecular sieve
With
dmap; palladium on activated charcoal; C30H40Br2ClFeN2O2; hydrogen; silver perchlorate; N-fluorobis(benzenesulfon)imide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1039/c4cc01631a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C / Inert atmosphere
2: N-fluorobis(benzenesulfon)imide; silver perchlorate; C30H40Br2ClFeN2O2 / diethyl ether / 8 h / 0 °C / Inert atmosphere; Molecular sieve
With
palladium on activated charcoal; C30H40Br2ClFeN2O2; hydrogen; silver perchlorate; N-fluorobis(benzenesulfon)imide;
In
methanol; diethyl ether;
DOI:10.1039/c4cc01631a