C₂₈H₂₈FN₃O₅S

Base Information

Chemical Name:C₂₈H₂₈FN₃O₅S
CAS No.:1093121-03-9
Molecular Formula:C₂₈H₂₈FN₃O₅S
Molecular Weight:537.612
Hs Code.:

C<sub>28</sub>H<sub>28</sub>FN<sub>3</sub>O<sub>5</sub>S

Synonyms:C₂₈H₂₈FN₃O₅S

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Chemical Property of C₂₈H₂₈FN₃O₅S

Chemical Property:

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Technology Process of C₂₈H₂₈FN₃O₅S

There total 8 articles about C₂₈H₂₈FN₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 915948-89-9
3-((S)-2-methoxy-1-methyl-ethoxy)-5-((S)-1-methyl-2-phenyl-ethoxy)-benzoic acid

: 1001327-31-6
C₈H₆FN₃OS

: 1093121-03-9
C₂₈H₂₈FN₃O₅S

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

Reference yield:

: 851885-42-2
methyl 3-{[(1S)-1-methyl-2-(methyloxy)ethyl]oxy}-5-[(phenylmethyl)oxy]benzoate

: 1093121-03-9
C₂₈H₂₈FN₃O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 12 h / 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12.08 h / 0 - 20 °C

3.1: lithium hydroxide; water / tetrahydrofuran / 7 h / 20 - 45 °C

3.2: pH 2

4.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; di-isopropyl azodicarboxylate; water; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1093121-03-9
C₂₈H₂₈FN₃O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12.17 - 18.5 h / 20 - 25 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 48 h / 0 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 12 h / 20 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12.08 h / 0 - 20 °C

5.1: lithium hydroxide; water / tetrahydrofuran / 7 h / 20 - 45 °C

5.2: pH 2

6.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; di-isopropyl azodicarboxylate; water; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;