2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester

Base Information

Chemical Name:2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester
CAS No.:1370252-63-3
Molecular Formula:C₁₈H₁₈N₂O₄
Molecular Weight:326.352
Hs Code.:

Synonyms:2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester

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Chemical Property of 2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester

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Technology Process of 2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester

There total 1 articles about 2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 272-49-1
1H-pyrrolo[3,2-b]pyridine

: 1071973-76-6
4-fluoro-2-methoxymethoxy-benzoic acid ethyl ester

: 1370252-63-3
2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 - 80 ℃;

Reference yield:

: 1370252-63-3
2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester

: 1370252-65-5
4-(3-bromopyrrolo[3,2-b]pyridine-1-yl)-2-methoxymethoxy benzoic acid ethyl ester

Guidance literature:: With N-Bromosuccinimide; In dichloromethane; for 2h; Cooling with ice;

Reference yield:

: 1370252-63-3
2-methoxymethoxy-4-pyrrolo[3,2-b]pyridine-1-yl-benzoic acid ethyl ester

: 1370252-33-7
4-(3-cyanopyrrolo[3,2-b]pyridine-1-yl)-2-hydroxy-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / 2 h / Cooling with ice

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1-methyl-pyrrolidin-2-one / 1 h / 20 - 150 °C / Microwave irradiation

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water; ethanol / 5 h / 20 °C

3.2: 50 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium hydroxide monohydrate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; water;