C₃₇H₇₂O₆Si₃

Base Information

Chemical Name:C₃₇H₇₂O₆Si₃
CAS No.:1402659-45-3
Molecular Formula:C₃₇H₇₂O₆Si₃
Molecular Weight:697.232
Hs Code.:

C<sub>37</sub>H<sub>72</sub>O<sub>6</sub>Si<sub>3</sub>

Synonyms:C₃₇H₇₂O₆Si₃

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Chemical Property of C₃₇H₇₂O₆Si₃

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Technology Process of C₃₇H₇₂O₆Si₃

There total 1 articles about C₃₇H₇₂O₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254369-15-7
C₄₀H₇₅NO₇Si₃

: 100-51-6,185532-71-2
benzyl alcohol

: 1402659-45-3
C₃₇H₇₂O₆Si₃

Guidance literature:: benzyl alcohol; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

C₄₀H₇₅NO₇Si₃; In tetrahydrofuran; hexane; at -45 - 20 ℃; for 7h;
DOI:10.1021/ml300230h

Reference yield: 85.0%

: 1402659-45-3
C₃₇H₇₂O₆Si₃

: 1402659-46-4
C₂₅H₄₄O₆Si

Guidance literature:: With camphor-10-sulfonic acid; In methanol; at 0 ℃; for 1h;
DOI:10.1021/ml300230h

Reference yield:

: 1402659-45-3
C₃₇H₇₂O₆Si₃

: C₄₁H₇₀Cl₃NO₁₁Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: camphor-10-sulfonic acid / methanol / 1 h / 0 °C

2: 1H-imidazole / dichloromethane / 3 h / 20 °C

3: silver trifluoromethanesulfonate; 2,6-di-tert-butyl-4-methylpyridine / dichloromethane; toluene / 20 h / 0 - 20 °C / Molecular sieve

4: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate

5: triethylamine / tetrahydrofuran / 3 h / 20 °C

With 1H-imidazole; 2,6-di-tert-butyl-4-methylpyridine; palladium 10% on activated carbon; camphor-10-sulfonic acid; hydrogen; silver trifluoromethanesulfonate; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; toluene;
DOI:10.1021/ml300230h