Technology Process of C28H29N3O4
There total 4 articles about C28H29N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 20 ℃;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / 5 % platinum on carbon / tetrahydrofuran; methanol / 50 °C
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; N,N-dimethyl-formamide / 20 °C / Molecular sieve
With
hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
5 % platinum on carbon;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / dichloromethane / 21 h
2: hydrogen / 5 % platinum on carbon / tetrahydrofuran; methanol / 50 °C
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; N,N-dimethyl-formamide / 20 °C / Molecular sieve
With
hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
5 % platinum on carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;