C₁₆H₁₈SiC₈H₁₂O₂CH₂O

Base Information

Chemical Name:C₁₆H₁₈SiC₈H₁₂O₂CH₂O
CAS No.:954145-02-9
Molecular Formula:C₂₅H₃₂O₃Si
Molecular Weight:408.613
Hs Code.:

C<sub>16</sub>H<sub>18</sub>SiC<sub>8</sub>H<sub>12</sub>O<sub>2</sub>CH<sub>2</sub>O

Synonyms:C₁₆H₁₈SiC₈H₁₂O₂CH₂O

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Chemical Property of C₁₆H₁₈SiC₈H₁₂O₂CH₂O

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Technology Process of C₁₆H₁₈SiC₈H₁₂O₂CH₂O

There total 8 articles about C₁₆H₁₈SiC₈H₁₂O₂CH₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 954145-08-5
C₁₆H₁₈SiC₈H₁₂O₂CH₂H₂O

: 954145-02-9
C₁₆H₁₈SiC₈H₁₂O₂CH₂O

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/ol701783z

Reference yield:

: 954144-99-1
C₁₀H₁₄O₃

: 954145-02-9
C₁₆H₁₈SiC₈H₁₂O₂CH₂O

Guidance literature:: Multi-step reaction with 8 steps

1.1: 87 percent / urea hydrogen peroxide complex; trifluoroacetic anhydride / CH₂Cl₂ / 5 h / 0 °C

2.1: 88 percent / K₂CO₃ / methanol; H₂O / 20 h / 20 °C

3.1: 100 percent / imidazole / dimethylformamide / 36 h / 20 °C

4.1: tetrahydrofuran; toluene / 3 h / 90 °C

5.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 1 h / 0 - 20 °C

5.2: 766.8 mg / NaOH; H₂O₂ / tetrahydrofuran; H₂O / 0 - 20 °C

6.1: 98 percent / imidazole / dimethylformamide / 3 h / 20 °C

7.1: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / tetrahydrofuran; H₂O / 36 h / 20 °C

8.1: 96 percent / DMSO; oxalyl chloride; triethylamine / CH₂Cl₂ / -78 - 20 °C

With 1H-imidazole; oxalyl dichloride; urea hydrogen peroxide; potassium carbonate; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; trifluoroacetic anhydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1.1: Baeyer-Villiger oxidation / 4.1: Petasis olefination / 8.1: Swern oxidation;
DOI:10.1021/ol701783z

Reference yield:

: C₆H₁₄SiC₈H₁₂O₂CH₂

: 954145-02-9
C₁₆H₁₈SiC₈H₁₂O₂CH₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 766.8 mg / NaOH; H₂O₂ / tetrahydrofuran; H₂O / 0 - 20 °C

2.1: 98 percent / imidazole / dimethylformamide / 3 h / 20 °C

3.1: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / tetrahydrofuran; H₂O / 36 h / 20 °C

4.1: 96 percent / DMSO; oxalyl chloride; triethylamine / CH₂Cl₂ / -78 - 20 °C

With 1H-imidazole; oxalyl dichloride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 4.1: Swern oxidation;
DOI:10.1021/ol701783z