(S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

Base Information

Chemical Name:(S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide
CAS No.:128781-64-6
Molecular Formula:C₁₃H₁₃F₃N₂O₄S
Molecular Weight:350.318
Hs Code.:

Synonyms:(S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

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Technology Process of (S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

There total 5 articles about (S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 128781-60-2
(S)-N-<<3-<4-<(trifluoromethyl)thio>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

: 128781-64-6
(S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 60h; Ambient temperature;
DOI:10.1021/jm00171a035

Reference yield:

: 96800-17-8
(S)-N-<<3-phenyl-2-oxo-5-oxazolidinyl>methyl>acetamide

: 128781-64-6
(S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / chlorosulfuric acid / 1 h / Ambient temperature

2: 79 percent / Zn, acetic acid, sodium acetate / 1 h / Heating

3: 100 percent / pyrrolidine / ethanol

4: 33 percent / liq. NH₃ / 1 h / -33 °C / Irradiation

5: 66 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 60 h / Ambient temperature

With pyrrolidine; chlorosulphuric acid; ammonia; sodium acetate; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In ethanol; dichloromethane;
DOI:10.1021/jm00171a035

Reference yield:

: 96800-01-0
(S)-N-<<3-(4-mercaptophenyl)-2-oxo-5-oxazolidinyl>methyl>acetamide

: 128781-64-6
(S)-N-<<3-<4-<(trifluoromethyl)sulfinyl>phenyl>-2-oxo-5-oxazolidinyl>methyl>acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / liq. NH₃ / 1 h / -33 °C / Irradiation

2: 66 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 60 h / Ambient temperature

With ammonia; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00171a035