2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

Base Information

Chemical Name:2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine
CAS No.:862490-75-3
Molecular Formula:C₂₉H₄₅N₅O₅Si₂
Molecular Weight:599.878
Hs Code.:

2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N<sub>6</sub>-benzyladenosine

Synonyms:2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

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Chemical Property of 2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

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Technology Process of 2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

There total 3 articles about 2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 862490-65-1
3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

: 862490-75-3
2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

Guidance literature:: With methanesulfonic acid; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;
DOI:10.1021/jo050205w

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 862490-75-3
2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / tetrahydrofuran / 8.17 h / 0 - 20 °C

2: 56 percent / methanesulfonic acid / dimethylformamide / 24 h / 0 - 20 °C

With pyridine; methanesulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo050205w

Reference yield:

: 4294-16-0
N₆-Benzyladenosine

: 862490-75-3
2',3'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-N₆-benzyladenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / tetrahydrofuran / 8.17 h / 0 - 20 °C

2: 56 percent / methanesulfonic acid / dimethylformamide / 24 h / 0 - 20 °C

With pyridine; methanesulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo050205w