Technology Process of C25H27NO2S
There total 5 articles about C25H27NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon;
In
ethyl acetate;
at 20 ℃;
for 10h;
DOI:10.1055/s-0030-1260974
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 1,2-dichloro-ethane / 5 h / 20 °C
2: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Reflux
3: palladium 10% on activated carbon / ethyl acetate / 10 h / 20 °C
With
pyridine; palladium 10% on activated carbon; boron trifluoride diethyl etherate;
In
dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1055/s-0030-1260974
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / methanol / 20 °C
2: pyridine / 1,2-dichloro-ethane / 5 h / 20 °C
3: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Reflux
4: palladium 10% on activated carbon / ethyl acetate / 10 h / 20 °C
With
pyridine; sodium tetrahydroborate; palladium 10% on activated carbon; boron trifluoride diethyl etherate;
In
methanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1055/s-0030-1260974