1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide

Base Information

Chemical Name:1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide
CAS No.:86956-41-4
Molecular Formula:C₁₉H₃₀ClN₃O₂
Molecular Weight:367.919
Hs Code.:

Synonyms:1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide

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Chemical Property of 1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide

Chemical Property:

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Technology Process of 1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide

There total 4 articles about 1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69082-74-2
4-Chloro-2-(4-pyridinecarboxamido)anisole hydrochloride

: 86956-41-4
1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / H₂ / PtO₂ / ethanol / 6 h / 70 °C / 15514.4 Torr

2: 82 percent / fuming HNO₃, H₂SO₄ / acetic acid / 2 h

3: K₂CO₃ / dimethylformamide / 16 h

4: SnCl₂, conc. HCl / acetic acid / Ambient temperature

With hydrogenchloride; sulfuric acid; hydrogen; nitric acid; potassium carbonate; tin(ll) chloride; platinum(IV) oxide; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00366a017

Reference yield:

: 1-Hexyl-piperidine-4-carboxylic acid (5-chloro-2-methoxy-4-nitro-phenyl)-amide

: 86956-41-4
1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide

Guidance literature:: With hydrogenchloride; tin(ll) chloride; In acetic acid; Yield given; Ambient temperature;
DOI:10.1021/jm00366a017

Reference yield:

: 69082-73-1
N-(5-chloro-2-methoxyphenyl)-4-piperidinecarboxamide

: 86956-41-4
1-Hexyl-piperidine-4-carboxylic acid (4-amino-5-chloro-2-methoxy-phenyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / fuming HNO₃, H₂SO₄ / acetic acid / 2 h

2: K₂CO₃ / dimethylformamide / 16 h

3: SnCl₂, conc. HCl / acetic acid / Ambient temperature

With hydrogenchloride; sulfuric acid; nitric acid; potassium carbonate; tin(ll) chloride; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00366a017