ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate

Base Information

Chemical Name:ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate
CAS No.:1610422-75-7
Molecular Formula:C₂₉H₃₁NO₄
Molecular Weight:457.569
Hs Code.:

Synonyms:ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate

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Chemical Property of ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate

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Technology Process of ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate

There total 3 articles about ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1610422-73-5
ethyl N-methyl-(2-((8-phenyl-9-(4-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy)phenyl)-6,7-dihydro-5H-benzocyclohepten-3-yl)oxy)ethyl)carbamate

: 1610422-75-7
ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate

Guidance literature:: With sodium methylate; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jm500569h

Reference yield:

: 113748-84-8
6,7-dihydro-8-phenyl-9-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-5H-benzocyclohepten-3-ol

: 1610422-75-7
ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 16 h / 20 °C / Inert atmosphere

2: sodium methylate / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

With sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm500569h

Reference yield:

: 113748-82-6
3-methoxy-6,7-dihydro-8-phenyl-9-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-5H-benzocycloheptene

: 1610422-75-7
ethyl (2-((9-(4-hydroxyphenyl)-8-phenyl-6,7-dihydro-5H-benzocycloehepten-3-yl)oxy)ethyl)(N-methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide; acetic acid / water / 10 h / Inert atmosphere; Reflux

2: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 16 h / 20 °C / Inert atmosphere

3: sodium methylate / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

With hydrogen bromide; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; acetic acid; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm500569h