1,1'-dibenzyl-5,5'-dimethoxy-1H,1'H-2,3'-biindole

Base Information

• Chemical Name: 1,1'-dibenzyl-5,5'-dimethoxy-1H,1'H-2,3'-biindole
• CAS No.: 1201825-39-9
• Molecular Formula: C₃₂H₂₈N₂O₂
• Molecular Weight: 472.587
• Mol file: 1201825-39-9.mol

Synonyms:1,1'-dibenzyl-5,5'-dimethoxy-1H,1'H-2,3'-biindole

Chemical Property of 1,1'-dibenzyl-5,5'-dimethoxy-1H,1'H-2,3'-biindole

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1,1'-dibenzyl-5,5'-dimethoxy-1H,1'H-2,3'-biindole

There total 1 articles about 1,1'-dibenzyl-5,5'-dimethoxy-1H,1'H-2,3'-biindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-benzyl-5-methoxyindole (16382-21-1) → 1,1'-dibenzyl-5,5'-dimethoxy-1H,1'H-2,3'-biindole (1201825-39-9)

Guidance literature:

With palladium(II) trifluoroacetate; copper(II) acetate monohydrate; In dimethyl sulfoxide; at 20 ℃; for 8h; regioselective reaction; Inert atmosphere;

DOI:10.1021/jo902265s

upstream raw materials:

1-benzyl-5-methoxyindole

Refernces

• 1、 Liang, Zunjun,Zhao, Jinlong,Zhang, Yuhong. "Palladium-catalyzed regioselective oxidative coupling of indoles and one-pot synthesis of acetoxylated biindolyls". supporting information; experimental part. p. 170 - 177. Retrieved 2010/04/04.