2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester

Base Information

Chemical Name:2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester
CAS No.:181931-47-5
Molecular Formula:C₂₀H₃₀FO₆PS
Molecular Weight:448.493
Hs Code.:

Synonyms:2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester

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Chemical Property of 2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester

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Technology Process of 2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester

There total 6 articles about 2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 181931-47-5
2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / piperidine, acetic acid / benzene / 48 h / Heating

2: Et₃N / tetrahydrofuran / 24 h / Ambient temperature

3: 1.) oxalyl chloride, dimethyl sulfoxide, 3.) Et₃N

With piperidine; oxalyl dichloride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; benzene;
DOI:10.1002/jhet.5570330328

Reference yield:

: 456-04-2
2-Chloro-4'-fluoroacetophenone

: 181931-47-5
2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / ethanol / 24 h / Ambient temperature

2: LiAlH₄ / tetrahydrofuran / 1 h / Ambient temperature

3: Et₃N / tetrahydrofuran / 24 h / Ambient temperature

4: 1.) oxalyl chloride, dimethyl sulfoxide, 3.) Et₃N

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1002/jhet.5570330328

Reference yield:

: 181931-45-3
1-(4-Fluoro-phenyl)-2-mercapto-ethanol

: 181931-47-5
2-(Diethoxy-phosphoryl)-3-[2-(4-fluoro-phenyl)-2-oxo-ethylsulfanyl]-4-methyl-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 24 h / Ambient temperature

2: 1.) oxalyl chloride, dimethyl sulfoxide, 3.) Et₃N

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran;
DOI:10.1002/jhet.5570330328