(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid

Base Information

Chemical Name:(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid
CAS No.:1190373-32-0
Molecular Formula:C₃₈H₄₂O₈
Molecular Weight:626.747
Hs Code.:

Synonyms:(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid

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Chemical Property of (R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid

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Technology Process of (R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid

There total 1 articles about (R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1190373-30-8
(R)-methyl 3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoate

: 1190373-32-0
(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid

Guidance literature:: (R)-methyl 3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoate; With water; sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 24h;

With hydrogenchloride; water; In 1,4-dioxane;
DOI:10.1016/j.bmc.2009.06.016

Reference yield: 90.0%

: 1190373-32-0
(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid

: N-(adamantan-1-y)-L-alanyl-D-isoglutamine-5-amide trifluoroacetate

: N-(adamantan-1-yl)-[(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoyl]-L-alanyl-D-isoglutamine-5-amide

Guidance literature:: (R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; at 0 ℃; for 0.5h;

N-(adamantan-1-y)-L-alanyl-D-isoglutamine-5-amide trifluoroacetate; With triethylamine; In 1,4-dioxane; dichloromethane; water; at 0 - 20 ℃; for 49h;
DOI:10.3762/bjoc.15.174

Reference yield: 76.0%

: 1190373-32-0
(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid

: 1354546-12-5
(adamant-2-yl)glycyl-L-alanyl-D-isoglutamine tert-butyl ester

: 1354546-15-8
N-[(R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoyl]-(adamant-2-yl)glycyl-L-alanyl-D-isoglutamine tert-butyl ester

Guidance literature:: (R)-3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.5h;

(adamant-2-yl)glycyl-L-alanyl-D-isoglutamine tert-butyl ester; With triethylamine; In 1,4-dioxane; dichloromethane; at 0 - 20 ℃; for 49h;
DOI:10.5562/cca1827