C₅₁H₆₅NO₉Si

Base Information

Chemical Name:C₅₁H₆₅NO₉Si
CAS No.:532402-72-5
Molecular Formula:C₅₁H₆₅NO₉Si
Molecular Weight:864.164
Hs Code.:

C<sub>51</sub>H<sub>65</sub>NO<sub>9</sub>Si

Synonyms:C₅₁H₆₅NO₉Si

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Chemical Property of C₅₁H₆₅NO₉Si

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Technology Process of C₅₁H₆₅NO₉Si

There total 7 articles about C₅₁H₆₅NO₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532402-59-8
C₃₃H₃₈O₈

: 532402-72-5
C₅₁H₆₅NO₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 97 percent / Pd(dba)2*Ph₃P; HCOOH; NEt₃ / tetrahydrofuran / 48 h / Heating

2.1: 91 percent / OsO₄; 4-methylmorpholine N-oxide / tetrahydrofuran; H₂O / 120 h / 20 °C

3.1: CeCl₃*7H₂O; NaBH₄ / methanol / 0.5 h / 0 °C

3.2: 49 percent / NaIO₄ / tetrahydrofuran; H₂O / 3 h / 20 °C

4.1: 86 percent / imidazole / dimethylformamide / 4 h / 20 °C

5.1: 808 mg / NaBH₄ / methanol / 0.5 h / 0 °C

6.1: CF₃SOCl; DMAP / CH₂Cl₂ / 20 °C

6.2: tetrahydrofuran / 0.5 h / -78 °C

7.1: 95 percent / nBu₄NF / tetrahydrofuran / 0.08 h / 20 °C

8.1: 84 percent / (Me₃Si)2NNa / tetrahydrofuran / 0.33 h / -78 °C

With 1H-imidazole; trifluoracetyl chloride; dmap; sodium tetrahydroborate; osmium(VIII) oxide; formic acid; cerium(III) chloride; Pd(dba)2*Ph₃P; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200390109

Reference yield:

: 532402-61-2
C₂₄H₃₂O₆

: 532402-72-5
C₅₁H₆₅NO₉Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 91 percent / OsO₄; 4-methylmorpholine N-oxide / tetrahydrofuran; H₂O / 120 h / 20 °C

2.1: CeCl₃*7H₂O; NaBH₄ / methanol / 0.5 h / 0 °C

2.2: 49 percent / NaIO₄ / tetrahydrofuran; H₂O / 3 h / 20 °C

3.1: 86 percent / imidazole / dimethylformamide / 4 h / 20 °C

4.1: 808 mg / NaBH₄ / methanol / 0.5 h / 0 °C

5.1: CF₃SOCl; DMAP / CH₂Cl₂ / 20 °C

5.2: tetrahydrofuran / 0.5 h / -78 °C

6.1: 95 percent / nBu₄NF / tetrahydrofuran / 0.08 h / 20 °C

7.1: 84 percent / (Me₃Si)2NNa / tetrahydrofuran / 0.33 h / -78 °C

With 1H-imidazole; trifluoracetyl chloride; dmap; sodium tetrahydroborate; osmium(VIII) oxide; cerium(III) chloride; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200390109

Reference yield:

: 532402-64-5
C₂₃H₃₂O₇

: 532402-72-5
C₅₁H₆₅NO₉Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 86 percent / imidazole / dimethylformamide / 4 h / 20 °C

2.1: 808 mg / NaBH₄ / methanol / 0.5 h / 0 °C

3.1: CF₃SOCl; DMAP / CH₂Cl₂ / 20 °C

3.2: tetrahydrofuran / 0.5 h / -78 °C

4.1: 95 percent / nBu₄NF / tetrahydrofuran / 0.08 h / 20 °C

5.1: 84 percent / (Me₃Si)2NNa / tetrahydrofuran / 0.33 h / -78 °C

With 1H-imidazole; trifluoracetyl chloride; dmap; sodium tetrahydroborate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200390109