allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Base Information

Chemical Name:allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide
CAS No.:1393677-12-7
Molecular Formula:C₃₀H₃₅NO₄P*I
Molecular Weight:631.49
Hs Code.:

Synonyms:allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

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Chemical Property of allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Chemical Property:

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Technology Process of allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

There total 7 articles about allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1393677-11-6
allyl (S)-4-iodo-2-(N-tert-butyloxycarbonylamino)butanoate

: 603-35-0
triphenylphosphine

: 1393677-12-7
allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Guidance literature:: In neat (no solvent); at 80 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo3013622

Reference yield:

: 1393677-10-5
allyl (S)-4-iodo-2-[N,N-bis(tert-butyloxycarbonyl)amino]butanoate

: 1393677-12-7
allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Guidance literature:: Multi-step reaction with 2 steps

1: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 20 °C / Inert atmosphere

2: neat (no solvent) / 2 h / 80 °C / Inert atmosphere

With cerium(III) chloride heptahydrate; sodium iodide; In acetonitrile;
DOI:10.1021/jo3013622

Reference yield:

: 1393677-09-2
allyl (S)-2-(t-butyloxycarbonylamino)-3-(methoxycarbonyl)propanoate

: 1393677-12-7
allyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Guidance literature:: Multi-step reaction with 6 steps

1: dmap / acetonitrile / 20 °C / Inert atmosphere

2: diisobutylaluminium hydride / diethyl ether / 1 h / -78 °C / Inert atmosphere

3: sodium tetrahydroborate / tetrahydrofuran; water / 0.5 h / 0 °C / Inert atmosphere

4: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 20 °C / Inert atmosphere

6: neat (no solvent) / 2 h / 80 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium tetrahydroborate; cerium(III) chloride heptahydrate; iodine; diisobutylaluminium hydride; triphenylphosphine; sodium iodide; In tetrahydrofuran; diethyl ether; water; acetonitrile;
DOI:10.1021/jo3013622