2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal

Base Information

Chemical Name:2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal
CAS No.:127880-39-1
Molecular Formula:C₂₄H₂₄O₆
Molecular Weight:408.451
Hs Code.:

Synonyms:2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal

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Chemical Property of 2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal

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Technology Process of 2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal

There total 3 articles about 2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 106625-69-8
ethyl (E)-3-phenyl-2-propenyl carbonate

: 50-81-7,98966-42-8
ascorbic acid

: 127855-06-5
(E)-2-(3-phenylallyl)-3-oxo-L-gulonolactone 3,6-hemiketal

: 127880-39-1
2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal

Guidance literature:: With bis(acetylacetonato)palladium(II); triphenylphosphine; In tetrahydrofuran; for 3.5h; Product distribution; Heating; further reagents and allylic derivative investigated;
DOI:10.1021/jo00303a032

Reference yield: 16.0%

: 106625-69-8
ethyl (E)-3-phenyl-2-propenyl carbonate

: 15042-01-0
5,6-O-isopropylidene-L-ascorbic acid

: 2-cinnamyl-5,6-isopropylidene-L-ascorbic acid

: 127880-39-1
2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal

Guidance literature:: With bis(acetylacetonato)palladium(II); triphenylphosphine; In tetrahydrofuran; for 3.5h; Heating;
DOI:10.1021/jo00303a032

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 127880-39-1
2-(3-phenylallyl)-2-((3-phenylallyl)oxy)-3-oxo-L-gulonolactone 3,6-hemiketal

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0 - 10 °C

2: 16 percent / bis(pentane-2,4-dionato)palladium(II), triphenylphosphine / tetrahydrofuran / 3.5 h / Heating

With pyridine; bis(acetylacetonato)palladium(II); triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/jo00303a032