1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid

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Chemical Name:1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid
CAS No.:118964-87-7
Molecular Formula:C₂₅H₂₆N₄O₅S
Molecular Weight:494.571
Hs Code.:

Synonyms:1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid

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Chemical Property of 1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid

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Technology Process of 1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid

There total 5 articles about 1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 118964-61-7
1-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid; hydriodide

: 118964-64-0
1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid; hydriodide

: 118964-87-7
1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid

Guidance literature:: With ammonium acetate; In methanol; at 60 ℃; for 3h;

Reference yield:

: 147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7
L-proline

: 118964-87-7
1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / 2 M KOH / diethyl ether / 4 h

2: 65 percent / H₂S, TEA / pyridine / 72 h / Ambient temperature

3: 70 percent / acetone / 0.17 h / Heating

4: 90 percent / CH₃COONH₄ / methanol / 3 h / 60 °C

With potassium hydroxide; TEA; hydrogen sulfide; ammonium acetate; In pyridine; methanol; diethyl ether; acetone;

Reference yield:

: 80874-13-1
3-(4-Cyano-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl chloride

: 118964-87-7
1-[3-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-propionyl]-pyrrolidine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / 2 M KOH / diethyl ether / 4 h

2: 65 percent / H₂S, TEA / pyridine / 72 h / Ambient temperature

3: 70 percent / acetone / 0.17 h / Heating

4: 90 percent / CH₃COONH₄ / methanol / 3 h / 60 °C

With potassium hydroxide; TEA; hydrogen sulfide; ammonium acetate; In pyridine; methanol; diethyl ether; acetone;