3-Nitro-N-phenyl-4-quinolinamine

Base Information

Chemical Name:3-Nitro-N-phenyl-4-quinolinamine
CAS No.:99009-93-5
Molecular Formula:C₁₅H₁₁N₃O₂
Molecular Weight:265.271
Hs Code.:
DSSTox Substance ID:DTXSID901302452

Synonyms:3-Nitro-N-phenyl-4-quinolinamine;3-Nitro-N-phenylquinolin-4-amine;DTXSID901302452

Suppliers and Price of 3-Nitro-N-phenyl-4-quinolinamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Nitro-N-phenyl-4-quinolinamine

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:265.085126602
Heavy Atom Count:20
Complexity:339

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC2=C(C=NC3=CC=CC=C32)[N+](=O)[O-]

Technology Process of 3-Nitro-N-phenyl-4-quinolinamine

There total 4 articles about 3-Nitro-N-phenyl-4-quinolinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 39061-97-7
4-chloro-3-nitroquinoline

: 62-53-3
aniline

: 99009-93-5
3-nitro-N-phenylquinolin-4-amine

Guidance literature:: In methanol; at 80 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1039/c6ra15118c

Reference yield:

: 50332-66-6
3-nitro-quinolin-4-ol

: 99009-93-5
3-nitro-N-phenylquinolin-4-amine

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂; DMF / CH₂Cl₂ / 3 h / Heating

2: Et₃N / CH₂Cl₂ / Heating

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jm049211v

Reference yield:

: 611-36-9
quinolin-4-ol

: 99009-93-5
3-nitro-N-phenylquinolin-4-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / aq. HNO₃ / propionic acid / 0.25 h / 125 °C

2: SOCl₂; DMF / CH₂Cl₂ / 3 h / Heating

3: Et₃N / CH₂Cl₂ / Heating

With thionyl chloride; nitric acid; triethylamine; N,N-dimethyl-formamide; In dichloromethane; propionic acid;
DOI:10.1021/jm049211v