1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Base Information

• Chemical Name: 1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate
• CAS No.: 136185-90-5
• Molecular Formula: C₁₄H₂₀Cl₂N₃O₄P
• Molecular Weight: 396.21
• Mol file: 136185-90-5.mol

Synonyms:1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Chemical Property of 1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Chemical Property:

Purity/Quality:

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Technology Process of 1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

There total 1 articles about 1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H18Cl3N2O4P → 1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate (136185-90-5)

Guidance literature:

With ammonia; In tetrahydrofuran; hexane; at 0 ℃; Yield given;

DOI:10.1021/jm00114a013

Reference yield:

1-(4-nitrophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate (136185-90-5) → cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide (129253-32-3,136235-89-7)

Guidance literature:

With dihydrogen peroxide; ozone; Yield given. Multistep reaction; 1.) acetone, H₂O, 0 deg C, 2.) acetone, H₂O, RT, overnight;

DOI:10.1021/jm00114a013

Downstream raw materials:

cis-2--4-hydroperoxy-6-(4-nitrophenyl)tetrahydro-2H-1,3,2-oxazaphosphorine 2-oxide