Technology Process of C35H59N5O8
There total 14 articles about C35H59N5O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jm3009629
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
2.2: 12 h / 20 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
4.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
5.1: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
6.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
7.1: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1021/jm3009629
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1021/jm3009629