ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

Base Information

Chemical Name:ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate
CAS No.:1031337-97-9
Molecular Formula:C₃₂H₃₂N₄O₃
Molecular Weight:520.631
Hs Code.:

Synonyms:ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

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Chemical Property of ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

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Technology Process of ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

There total 2 articles about ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1031337-88-8
ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(3-oxospiro[3.5]non-1-en-1-yl)-L-phenylalaninate

: 65-85-0,8013-63-6
benzoic acid

: 1031337-97-9
ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

Guidance literature:: ethyl 4-[(3-aminopyridin-2-yl)amino]-N-(3-oxospiro[3.5]non-1-en-1-yl)-L-phenylalaninate; benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 18h;

With acetic acid; at 125 ℃; for 0.0833333h; Microwave irradiation;

With water; sodium hydrogencarbonate;

Reference yield:

: 1054611-45-8
C₃₂H₃₄N₄O₄

: 1031337-97-9
ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

Guidance literature:: With acetic acid; at 125 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1016/j.bmcl.2008.05.075

Reference yield: 18.0%

: 1031337-97-9
ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate

: 1031340-93-8
N-(2-bromo-3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalanine

Guidance literature:: ethyl N-(3-oxospiro[3.5]non-1-en-1-yl)-4-(2-phenyl-3H-imidazo[4,5-b]pyridin-3-yl)-L-phenylalaninate; With N-Bromosuccinimide; In ethyl acetate; at 20 ℃; for 16h;

With sodium hydroxide; water; In tetrahydrofuran; for 3h;

With hydrogenchloride; water; pH=4;