p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside

Base Information

Chemical Name:p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside
CAS No.:84564-28-3
Molecular Formula:C₄₆H₄₂N₂O₁₈
Molecular Weight:910.842
Hs Code.:

Synonyms:p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside

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Chemical Property of p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside

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Technology Process of p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside

There total 1 articles about p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 94062-91-6
p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-α-D-mannopyranoside

: 10028-45-2
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl bromide

: 84564-28-3
p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside

Guidance literature:: With mercury(II) cyanide; In acetonitrile; at 4 ℃; for 48h;
DOI:10.1016/0008-6215(82)85025-8

Reference yield:

: 84564-28-3
p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside

: 84594-50-3
Benzoic acid (2R,3S,4S,5R,6R)-3-[(2S,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-2-(4-nitro-phenoxy)-tetrahydro-pyran-4-yl ester

Guidance literature:: With acetic acid; at 100 ℃; for 0.25h;
DOI:10.1016/0008-6215(82)85025-8

Reference yield:

: 84564-28-3
p-nitrophenyl 3-O-benzoyl-4,6-O-benzylidene-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranoside

: C₁₈H₂₆N₂O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: 0.19 g / 80percent AcOH / 0.25 h / 100 °C

2: 85percent hydrazine hydrate / aq. ethanol / 1 h / Heating

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1016/0008-6215(82)85025-8