N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate

Base Information

• Chemical Name: N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate
• CAS No.: 83634-80-4
• Molecular Formula: C₇H₈O₃S*C₉H₂₁NO₃S
• Molecular Weight: 395.541
• Mol file: 83634-80-4.mol

Synonyms:N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate

Chemical Property of N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate

There total 2 articles about N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

toluene-4-sulfonic acid (104-15-4) + neopentyl 2-(dimethylamino)ethanesulfonate (75391-29-6) → N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate (83634-80-4)

Guidance literature:

In dichloromethane;

DOI:10.1021/ja00389a038

Reference yield:

2,2-dimethylpropyl ethenesulfonate (75391-24-1) → N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate (83634-80-4)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.17 h

2: 99 percent / CH₂Cl₂

In dichloromethane;

DOI:10.1021/ja00389a038

Reference yield: 2.0%

N,N-dimethyl-2-<(2,2-dimethylpropoxy)sulfonyl>ethanaminium p-toluenesulfonate (83634-80-4) → neopentyl tosylate (2346-07-8)

Guidance literature:

In toluene; at 110 ℃; for 24h;

DOI:10.1021/ja00389a038

upstream raw materials:

toluene-4-sulfonic acid

neopentyl 2-(dimethylamino)ethanesulfonate

2,2-dimethylpropyl ethenesulfonate

Downstream raw materials:

neopentyl tosylate