5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 ⁽⁵⁾-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester

Base Information

• Chemical Name: 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 ⁽⁵⁾-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester
• CAS No.: 672296-35-4
• Molecular Formula: C₃₈H₆₆O₇Si₂
• Molecular Weight: 691.109

Synonyms:5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 ⁽⁵⁾-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester

Chemical Property of 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 ⁽⁵⁾-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester

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Technology Process of 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 ⁽⁵⁾-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester

There total 1 articles about 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 ⁽⁵⁾-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(4R,5S,7S)-5,7-bis(tert-butyldimethylsilanyloxy)-4-methyl-8-oxooct-2-enoic acid ethyl ester (672296-34-3) + C33H35O3P → 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 (5)-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester (672296-35-4)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; for 4.33333h;

Reference yield:

5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-10 (5)-[2-(4-METHOXY-benzyl)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, 8-dienoic acid ethyl ester (672296-35-4) → C36H62O7Si2

Guidance literature:

With potassium hydroxide; water; In tetrahydrofuran; ethanol; for 6h; Heating / reflux;

upstream raw materials:

(4R,5S,7S)-5,7-bis(tert-butyldimethylsilanyloxy)-4-methyl-8-oxooct-2-enoic acid ethyl ester

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