2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Base Information

Chemical Name:2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate
CAS No.:1031364-95-0
Molecular Formula:C₂₇H₂₅NO₅
Molecular Weight:443.499
Hs Code.:

2'-(CH<sub>2</sub>CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Synonyms:2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

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Chemical Property of 2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

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Technology Process of 2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

There total 6 articles about 2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 5336-90-3
acridine-9-carboxylic acid

: 1031364-93-8
methyl 4-hydroxy-3-(2-methoxypropyl)-5-methylbenzoate

: 1031364-95-0
2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Guidance literature:: acridine-9-carboxylic acid; With pyridine; p-toluenesulfonyl chloride; Inert atmosphere;

methyl 4-hydroxy-3-(2-methoxypropyl)-5-methylbenzoate; at 20 ℃; for 72h;

Reference yield:

: 499-76-3
4-hydroxy-3-methylbenzoic acid

: 1031364-95-0
2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / 17 h / 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate / acetone / 3 h / Reflux; Inert atmosphere

3.1: N,N-diethylaniline / 8 h / 200 °C / Inert atmosphere

4.1: pyridine / 20 °C / Cooling with ice; Inert atmosphere

5.1: mercury(II) trifluoroacetate / 1 h / Cooling with ice; Inert atmosphere

5.2: Cooling with ice

6.1: pyridine; p-toluenesulfonyl chloride / Inert atmosphere

6.2: 72 h / 20 °C

With pyridine; thionyl chloride; mercury(II) trifluoroacetate; potassium carbonate; p-toluenesulfonyl chloride; N,N-diethylaniline; In acetone;

Reference yield:

: 42113-13-3
methyl 4-hydroxy-3-methylbenzoate

: 1031364-95-0
2'-(CH₂CH[OMe]Me)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetone / 3 h / Reflux; Inert atmosphere

2.1: N,N-diethylaniline / 8 h / 200 °C / Inert atmosphere

3.1: pyridine / 20 °C / Cooling with ice; Inert atmosphere

4.1: mercury(II) trifluoroacetate / 1 h / Cooling with ice; Inert atmosphere

4.2: Cooling with ice

5.1: pyridine; p-toluenesulfonyl chloride / Inert atmosphere

5.2: 72 h / 20 °C

With pyridine; mercury(II) trifluoroacetate; potassium carbonate; p-toluenesulfonyl chloride; N,N-diethylaniline; In acetone;