(2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

Base Information

Chemical Name:(2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole
CAS No.:170552-54-2
Molecular Formula:C₂₄H₂₃N₃O₅
Molecular Weight:433.464
Hs Code.:

Synonyms:(2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

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Chemical Property of (2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

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Technology Process of (2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

There total 5 articles about (2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 170300-08-0
(1S,3S,2'S)-1-<2'-benzyloxycarbonyl-2'-(benzyloxycarbonyl)amino>ethyl-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

: 170552-54-2
(2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

: 170300-17-1
(2S,5S,11bS)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

Guidance literature:: With trifluoroacetic acid; In toluene; for 4h; Yields of byproduct given; Heating;
DOI:10.1016/0040-4020(95)00402-T

Reference yield:

: 170300-17-1
(2S,5S,11bS)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

: 170552-54-2
(2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

Guidance literature:: With trifluoroacetic acid; In xylene; Heating;
DOI:10.1039/C39940000613

Reference yield:

: (S)-1-((S)-2-Benzyloxycarbonyl-2-benzyloxycarbonylamino-ethyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

: 170552-54-2
(2S,5S,11bR)-2-(benzyloxycarbonyl)amino-5-methoxycarbonyl-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indole

Guidance literature:: Multi-step reaction with 3 steps

1: xylene / 24 h / Heating

2: xylene / 24 h / Heating

3: CF₃COOH / xylene / Heating

With trifluoroacetic acid; In xylene;
DOI:10.1039/C39940000613